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Intelligent Electromagnetic Sensor Laboratories (iEMSL)

Texas A&M University College of Engineering
iEMSL material characterization setup with Keysight PNA and dielectric constant measurement equipment and QWED FPOR and SPDR. Keysight PNA-X VNA  screen displaying S-parameters during a Dk/Df test of a sample material.

Electromagnetic Material Characterization Measurement Services

Accurately measure dielectric constant (Dk) and loss tangent (Df) of your materials with  fast turnaround.

Request a Quote


The Intelligent Electromagnetic Sensor Laboratories (iEMSL) at Texas A&M University, in collaboration with QWED and Warsaw University of Technology, offers specialized material characterization services. We precisely evaluate how materials interact with electromagnetic fields, providing critical data on their properties to support researchers and industries in advanced design and innovation.

Our Core Capabilities & Instrumentation

We precisely measure fundamental electromagnetic properties of materials, including complex permittivity (ϵ=ϵ′−jϵ′′), which comprises the dielectric constant (dk or ϵr′​) and the loss tangent (df or tanδ=ϵ′′/ϵ′), as well as shielding effectiveness.

We specialize in the characterization of solid dielectrics and semiconductors, which are foundational to modern electronics, acting as insulators in capacitors, substrates for printed circuit boards, and critical high-frequency components. Accurate analysis of their electrical properties is vital for product development, quality control, and advanced material selection.

What We Measure: Material Categories and Capabilities

Solid Dielectrics

We characterize insulating materials essential for high-frequency electronics.

  • Parameters: Dk (Dielectric Constant), Df (Loss Tangent)
  • Frequency Coverage: 8–52.5 GHz (method-dependent)
  • Methods: WR-90 8-12 GHz, SPDR 10 GHz, FPOR 10–52.5 GHz

Semiconductors

Measurements focused on characterizing bulk and surface conductivity.
We can also measure film on film-on-substrate coatings.

  • Parameters: Dk (Dielectric Constant), Df (Loss Tangent),
    σ (Conductivity), ρ (Resistivity), Rs (Sheet Resistance, Ω/sq)
  • Frequency Coverage: 10 GHz
  • Methods: SPDR 10 GHz

Measurement Systems Overview

Our measurements utilize advanced Keysight PNA-X (up to 26.5 GHz) and Rohde & Schwarz ZVA (up to 67 GHz) vector network analyzers. By combining industry-leading commercial software with our specialized tools, we ensure precise control and extraction of critical material parameters, tailored to your specific requirements.

Our services leverage three primary measurement systems, each optimized for specific material types and frequency ranges. Refer to the table below for a quick comparison:

WR-90 Waveguide Transmission Line

Frequency Range:
8.2 – 12.4 GHz (X-Band)

Sample Requirements:
Length: 22.86 mm, Width: 10.16 mm, Thickness: 2 or 5 mm

Temperature:
Room to 100°C

Application & Specs:
Broadband technique, best for lossy MUTs and machineable solids. It allows high-precision characterization of solid material, measuring dielectric constant (ε’) and loss tangent (tan δ) as well as Shielding Effectiveness (SE) in standard microwave applications.


For more information and pricing

Split Post Dielectric Resonator (SPDR)

Frequency:
10 GHz

Sample Requirements:
Length: > 45 mm, Width: 45 – 90 mm, Thickness: < 0.95mm
Planar samples with clean edges

Temperature:
Room to 100 °C

Application & Specs:
Supporting the IPC 2.5.5.15 and IEC 61189-2-721 standards, this resonator based method is ideal for accurate characterization of thin dielectrics. Provides the highest sensitivity and ultra-high accuracy for measuring extremely low-loss materials. Essential for characterizing ceramics and specialized polymers used in high-Q resonant structures. Characterizes film-on-substrate coatings.

For more information and pricing

Fabry-Perot Open Resonator (FPOR)

Frequency Range:
10.2 – 52.5 GHz

Sample Requirements:
Diameter: 110 mm, Thickness: 1 µm – 3 mm
If anisotropic, specify in-plane axes

Temperature:
Room to 80 °C

Application & Specs:
Ideal for non-destructive, non-contact testing of large, flat material samples (e.g., substrates, composites). Offers high Q factor measurements across a wide frequency spectrum. Characterize in-plane anisotropy of dielectric sheets, polymers, glasses.

For more information and pricing

More details are provided below:

► WR-90 Waveguide Transmission Line (8.2 -12.4 GHz)

For solid, homogenous materials, the iEMSL can measure the complex permittivity (±5% accuracy) and shielding effectiveness (±1% accuracy) in the 8 – 12GHz (X-band) range. Samples must have rectangular dimensions of 22.86 mm x 10.16 mm, with a thickness of 2 or 5 mm.

WR-90 Waveguide transmission line fixture sample size for Dk and shielding effectiveness measurement at 8-12 GHz (X Band).
WR-90 Waveguide transmission line fixture for Dk and shielding effectiveness measurement at 8-12 GHz.

The iEMSL utilizes the PNA-X Vector Network Analyzer for S-parameter extraction, the WR-90 waveguide and short plate, calibration to isolate the material, and a Nicholson-Ross-Weir extraction algorithm script to visualize your material’s response. You must provide a solid material matching the provided waveguide dimensions and a WR-90 spacer to tightly house the sample. The measurement accuracy of Dielectric constant is ±5% and for Shielding effectiveness is ±1%.

Price per Sample:

  • Room Temperature: $250 first + $100 additional
  • Up to 100°C: $400/sample

What you receive:

  • Extracted parameters (Dk, Df, SE, etc.)
  • Charts and tables (vs frequency and/or temperature as applicable)
  • Raw data (Touchstone files) on request
  • Technical Report on request (for extra charge)

View our example measurements.


► Split Post Dielectric Resonator (10 GHz) – in collaboration with QWED

The split post dielectric resonator (SPDR) can measure the dielectric constant and loss tangent of dielectric sheets. Samples must have a diameter between 45 mm and 90 mm and a thickness between 15 µm and 0.95 mm.

Split Post Dielectric Resonator (SPDR) used for precise 10 GHz Df and Dk test of thin dielectric sheets.

Utilizing the PNA-X Vector Network Analyzer, the iEMSL offers single frequency measurements of the dielectric constant at 10GHz with the SPDR. Supporting the IPC 2.5.5.15 and IEC 61189-2-721 standards, this resonator based method is ideal for accurate characterization of thin dielectrics. The measurement accuracy for Dielectric constant: is Δε/ε = ±(0.0015 + Δh/h) and for Loss tangent: Δtanδ = ±2×10⁻⁵ or ±0.03*tanδ (higher of the two). For more information, visit QWED.

Price per Sample:

  • Room Temperature: $250 first + $100 additional
  • Up to 100°C: $400/sample

What you receive:

  • Extracted parameters (Dk, Df, Rs, σ/ρ) and resonance/Q data
  • Charts and tables (vs frequency and/or temperature as applicable)
  • Raw data (CSV) on request
  • Technical Report on request (for extra charge)

View our example measurements.

► Fabry-Perot Open Resonator (10.2 – 52.2 GHz) – in collaboration with QWED

iEMSL utilizes the ZVA67 Vector Network Analyzer along with the FPOR to offer very high precision for dielectric constant (±0.25%) and loss tangent (±2%) measurements over the wide frequency band of 10 – 50GHz, the FPOR is ideal for a wide variety of measurements and precision needs. This also enables In-plane anisotropy testing and climatic compensation is always enabled. Samples should have a diameter between 75 mm and 110 mm and a thickness between 1 µm and 3 mm. The measurement accuracy for Dielectric constant: is ±0.25% (for Dk = 1 – 15) and for Loss tangent: tanδ < 10, ±2% (for Df >5×10⁻⁶).

Fabry-Perot Open Resonator (FPOR) setup for wideband complex dielectric measurement up to 52.2 GHz.

Thickness & Dk Limitations

This graph illustrates the relationship between a material’s dielectric constant (Dk) and its thickness, defining the measurable and unmeasurable regions for a specific testing method. The green and tan areas represent valid combinations that can be measured, while the two “prohibited zones” indicate combinations that cannot be reliably tested. For Dk < 3, the maximum thickness is 3mm.

  • Green Zone: This is the ideal measurement range, where combinations of Dk and thickness allow for highly reliable and precise results with a low measurement uncertainty of ±0.25%.
  • Tan Zone: This area indicates that a measurement can still be obtained, but with a greater uncertainty of ±0.5%.
  • Prohibited Zones: These zones represent invalid combinations of Dk and thickness where no reliable data can be acquired.
Graph illustrating the valid measurement ranges (Green and Tan Zones) for dielectric constant (Dk) versus sample thickness.

Thickness & Df Limitations

Limitations are imposed on the maximum loss tangent with respect to thickness. If the material has a very high loss, the resonator curve may not be distinguishable from noise.

Graph illustrating the limitations on maximum loss tangent (Df) measurement accuracy relative to sample thickness.

Dimension Requirements

To achieve the full frequency range down to 10.2 GHz, the target sample size should be between 101 mm and 109 mm. For rectangular samples, one dimension can be up to 150 mm, but the other must be less than 110 mm.

Holder dimensions for Fabry-Perot Open Resonator (FPOR) setup for wideband complex dielectric measurement up to 52.2 GHz.

Price per Sample:

  • Room Temperature: $450 first + $250 additional
  • Up to 80°C: $600/sample

What you receive:

  • Technical Report on request (for extra charge)
  • Extracted parameters (Dk, Df) and resonance/Q data
  • Charts and tables (vs frequency and/or temperature as applicable)
  • Raw data (CSV) on request
  • Technical Report on request (for extra charge)

View our example measurements.

Summary

Measurement System Frequency Range Applications Sample Requirements Price per Sample
Transmission Line
WR-90 Waveguide
8.2 – 12.4 GHz
(X-band)
Shielding Effectiveness (SE) testing

Permittivity of high-loss solids

Loss tangent of high-loss materials
Length: 22.86 mm
Width: 10.16 mm
Thickness: 2 or 5 mm
Room Temperature:
$250 first + $100 additional

Up to 100°C:
$400/sample
Split Post Dielectric Resonator
(SPDR)
10 GHz Complex permittivity of dielectric sheets

Supports IPC 2.5.5.15  & IEC 61189-2-721 standards

Characterizes film-on-substrate coatings by tracking tiny shifts in resonance frequency and Q-factor
Length: > 45 mm
Width: 45 – 90 mm
Thickness: < 0.95mm
Room Temperature:
$250 first + $100 additional

Up to 100°C:
$400/sample
Fabry-Perot Open Resonator
(FPOR)
10.2 – 52.2 GHz Wideband complex permittivity

In-plane anisotropy of dielectric sheets, polymers, glasses
Diameter: 101- 110 mm

Thickness: 1 µm – 3 mm
Room Temperature:
$450 first + $250 additional

Up to 80°C:
$600/sample
Note: TAMU researchers receive a 50% reduction on the listed prices.

Custom Solutions

Beyond our standard services, we provide custom solutions tailored to unique material characterization needs. Reach out, and we’ll strive to accommodate your request with our flexible, innovative approach. We can accomodate conductors, ferromagnetics, absorbers and liquids.

Ready to Measure?

iEMSL is equipped to support your material electrical testing needs. Click below to submit a request to have your material evaluated in our state-of-the-art facilities.

Request A Quote
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Intelligent Electromagnetic Sensor Laboratories (iEMSL)
Texas A&M University

188 Bizzell St,
College Station, Texas, USA 77843

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